Agilent 1260 LC [Agilent OpenLAB C.01.02 (中文)] 现场培训教材

仪器资料 · 发表于 2018-7-21 18:23:56

一、目录
二、培训目的 ................................................................................................................................. 3
三、培训准备 ................................................................................................................................. 3
1. 仪器准备 ................................................................................................................................. 3
2. 溶剂准备 ................................................................................................................................. 3
四、方法建立 ................................................................................................................................. 3
1. 开机准备 ................................................................................................................................. 3
2. 数据采集方法编辑 ................................................................................................................. 9
G1310A(单元泵) ...................................................................................................................... 9
G1312X(二元泵)/G1311X(四元泵) ........................................................................................ 10
G1313A(标准型自动进样器)，G1329B(自动控温自动进样器) ......................................... 11
G1367E(高性能自动进样器) ................................................................................................. 12
G1328A(手动进样器) ............................................................................................................ 14
G1316A/C (柱温箱) ............................................................................................................... 15
G1314BC/E/F(可变波长紫外检测器) ................................................................................... 15
G1315C/D ,G4212A/B(二极管阵列检测器)/ G1365C/D(多波长紫外检测器) ..................... 17
G1362A(示差检测器) ............................................................................................................ 18
G1321A(荧光检测器) ............................................................................................................ 19
G4218A(蒸发光散射检测器) ................................................................................................ 21
3. 数据分析方法编辑 ............................................................................................................... 22
谱图优化 ............................................................................................................................... 22
积分参数优化 ....................................................................................................................... 23
校正 ....................................................................................................................................... 25
打印报告 ............................................................................................................................... 27
光谱 ....................................................................................................................................... 28
4. 建立全新完整方法向导........................................................................................................ 30
5. 进样 ....................................................................................................................................... 30
单针进样 ............................................................................................................................... 30
序列进样 ............................................................................................................................... 31
五、关机 ....................................................................................................................................... 33
1. 关闭检测器的灯 ................................................................................................................... 33
2. 冲洗系统 ............................................................................................................................... 33
3. 封存色谱柱 ........................................................................................................................... 33
4. 关闭电脑 ............................................................................................................................... 33
5. 关闭模块 ............................................................................................................................... 33
六、 RRLC(快速液相)注意事项 ..................................................................................................... 33
七、特殊检测器的注意事项........................................................................................................ 35
八、 Agilent 1260 常见问题解决方法 .......................................................................................... 37
附一、维护知识 ............................................................................................................................... 39
附二、注册OpenLAB CDS 许可证的流程 ...................................................................................... 41