近红外书籍推荐：《hand of Near -Infrared Analysis》第三版
这个是国外的近红外手册，非常不错的一本书了，值得做近红外的朋友好好阅读阅读
作者：Donald A. Burns & Emil W. Ciurczak
Near-Infrared (NIR) spectroscopy is a technique whose time has arrived. And for good reason—it is
unusually fast compared to other analytical techniques (often taking less than 1 s), it is nondestructive,
and as often as not, no sample preparation is required. It is also remarkably versatile: if samples
contain such bonds as C−−H, N−−H, or O−−H, and if the concentration of the analyte exceeds about
0.1% of the total composition, then it is very likely to yield acceptable answers, even in the hands
of relatively untrained personnel.
The price to be paid, however, is the preliminary work, which is typical of any chemometric
method. The instrument/computer system must be “taught” what is important in the sample. While
this task may be time-consuming, it is not difficult. Today’s sophisticated software offers the user
such choices of data treatments as multiple linear regression (MLR), partial least squares (PLS),
principal components regression (PCR), factor analysis (FA), neural networks (NN), and Fourier
transform (FT), among others. The trade-off is a good one: even after several hours (or days) of
calibrating, the multiple advantages of analysis by NIR far outweigh the time required for method
development.
This book is divided into four parts. Following the Introduction and Background, there is a
general section on Instrumentation and Calibration. This is followed by Methods Development, and
the depth of NIR’s utility is covered by a broad (if not comprehensive) section on Applications.
The Handbook of Near-Infrared Analysis was written for practicing chemists and spectroscopists
in analytical, polymer, forage, baking, dairy products, petrochemicals, beverages, pharmaceutical,
and textile chemistry who are responsible for methods development or routine analyses where speed,
accuracy, and cost are vital factors.
Chapters 2 and 3 have been replaced (Basic Principles and Theories of Diffuse Reflection),
several chapters (4,19,25,26,29, and 37) have been updated (Commercial Instrumentation,
Analyses of Textiles and of Baked Products, Advances in the Petrochemical Industry,
Polymers, Pharmaceutical Applications, and Process Analysis), and some new chapters
(12,18,21,28,29,31,32,33,35, and 38) have been added (Process Sensors, Agro-Forestry Systems,
Gas Analysis, Use of NIR at the Bowling Alley, PAT in the Pharmaceutical Industry,
Nutraceuticals, Detection of Counterfeit Drugs (e.g., Viagra), NIR Photography in Medicine,
Biomedical Components in Blood and Serum, and The Detection of Counterfeit Currency and
Turquoise).
All this should enable you to assess the potential of NIR for solving problems in your own field
(and it could even lead to becoming a hero within your organization). You will discover the relative
merits of on-line, in-line, and at-line analyses for process control.You will see how interferences can
be removed spectrally rather than physically, and how to extract “hidden” information via derivatives,
indicator variables, and other data treatments.
Thanks are due to many people in our lives (i) Linda Burns, who put up with the disappearance
of all flat surfaces in our house for those weeks (or was it months?) when piles of
papers were everywhere, awaiting some semblance of organization into a book, (ii) the publisher,
whose prodding was minimal and whose patience was long, (iii) the special people in my (Emil’s)
life: Alissa, Alex, Adam, Alyssa, and Button (the Wonder Dog), and (iv) the many contributors,
both original and new. We hope that this general book will be useful to those already using
NIR as well as to those just entering the field and having to make important decisions regarding
instrumentation, software, and personnel. Suggestions for improving the next edition are most
welcome.
Donald A. Burns
Emil W. Ciurczak
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