Agilent Infinity II 6224-6230 Series TOF On-site现场培训手册

仪器资料 · 发表于 2019-5-12 16:49:05

版本 ......................................................................................................................................................................... 2
目录 ......................................................................................................................................................................... 3
1. 基本原理 ............................................................................................................................................................... 6
1.1 TOF的基本原理 ...................................................................................................................................................... 6
1.2 离子源技术和原理 ................................................................................................................................................. 7
1.2.1 ESI源—大气压电喷雾离子源 ......................................................................................................................... 7
1.2.2 APCI源—大气压化学电离离子源 ................................................................................................................... 7
1.2.3 ESI with Agilent Jet Steam Technology—带有安捷伦喷射流技术的ESI源 .................................................... 8
1.3不同离子源的比较 ................................................................................................................................................. 8
2. 硬件概览 ............................................................................................................................................................... 9
2.1典型配置图 ............................................................................................................................................................. 9
2.2仪器序列号位置 ..................................................................................................................................................... 9
2.3系统结构图示意图 ............................................................................................................................................... 10
3. 开机和关机 ..........................................................................................................................................................11
3.1 开机步骤 ............................................................................................................................................................... 11
3.2 关机步骤 ............................................................................................................................................................... 14
4. 软件概览 ..............................................................................................................................................................15
4.1 桌面常用软件图标介绍 ....................................................................................................................................... 15
4.2 软件功能区、状态区及快捷方式介绍 ................................................................................................................ 16
4.2.1 软件功能区与状态区 .................................................................................................................................... 16
4.2.2自动进样器的配置和快捷控制功能 ............................................................................................................. 18
4.2.3 泵的快捷控制功能 ........................................................................................................................................ 22
4.2.4 柱温箱的快捷控制功能 ................................................................................................................................ 23
4.2.5 DAD的快捷控制功能 ................................................................................................................................... 23
4.2.6 VWD的快捷控制功能 .................................................................................................................................. 24
4.2.7 TOF的快捷控制功能 ......................................................................................................................................... 25
5. 调谐和校正 ..........................................................................................................................................................25
5.1配制调谐液 ........................................................................................................................................................... 25
5.2 自动调谐介绍和比较 ........................................................................................................................................... 27
5.3 调谐界面功能概述 ............................................................................................................................................... 27
5.3.1 Manual Tune .................................................................................................................................................. 27
5.3.2 Diagnostics ..................................................................................................................................................... 28
5.3.3 Instrument State ............................................................................................................................................ 28
5.3.4 Preferences ..................................................................................................................................................... 28
5.4 INITIAL TUNE ............................................................................................................................................................. 29
5.5 STANDARD TUNE ........................................................................................................................................................ 30
5.6 QUICK TUNE .............................................................................................................................................................. 30
5.7 CHECK TUNE .............................................................................................................................................................. 30
5.8 CALIBRATION ............................................................................................................................................................. 31
5.9 保存调谐结果，返回采集界面 ............................................................................................................................ 32
6. 方法编辑 ..............................................................................................................................................................33
6.1 PROPERTIES ............................................................................................................................................................... 33
6.2 液相参数设置 ....................................................................................................................................................... 33
6.2.1自动进样器方法的设置 ................................................................................................................................ 33
6.2.1.1 G7167A/B Multisamlper自动进样器的方法设置 ...................................................................................... 33
6.2.1.2 G7129A/B Vialsampler自动进样器的方法设置 ........................................................................................ 35