【电子书】Chiral Separations：Methods and Protocols 手性分离：方法与原则
Chiral Separations
Methods and Protocols
Edited by
Gerald Gübitz
and
Martin G. Schmid
Institute of Pharmaceutical Chemistry and Pharmaceutical Technology,
Karl-Franzens University, Graz, Austria
Contents
Preface .............................................................................................................v
Contributors ..................................................................................................... xi
1 Chiral Separation Principles: An Introduction
Gerald Gübitz and Martin G. Schmid .................................................. 1
2 Separation of Enantiomers by Thin-Layer Chromatography:
An Overview
Kurt Günther, Peter Richter, and Klaus Möller ................................ 29
3 Cyclodextrin-Based Chiral Stationary Phases
for Liquid Chromatography: A Twenty-Year Overview
Clifford R. Mitchell and Daniel W. Armstrong .................................. 61
4 Enantiomeric Separations by HPLC Using Macrocyclic
Glycopeptide-Based Chiral Stationary Phases:
An Overview
Tom Ling Xiao and Daniel W. Armstrong ....................................... 113
5 Chiral Separation by HPLC Using Polysaccharide-Based
Chiral Stationary Phases
Chiyo Yamamoto and Yoshio Okamoto.......................................... 173
6 Applications of Polysaccharide-Based Chiral Stationary Phases
for Resolution of Different Compound Classes
Hassan Y. Aboul-Enein and Imran Ali ............................................. 183
7 Chiral Separation by HPLC With Pirkle-Type
Chiral Stationary Phases
Myung Ho Hyun and Yoon Jae Cho ................................................ 197
8 Chiral Separation by HPLC Using the Ligand-Exchange Principle
Vadim A. Davankov ........................................................................... 207
9 Chiral Separations by HPLC Using Molecularly Imprinted Polymers
Peter Spégel, Lars I. Andersson, and Staffan Nilsson ................. 217
10 Indirect Enantioseparation by HPLC Using Chiral
Benzofurazan-Bearing Reagents
Toshimasa Toyo'oka ......................................................................... 231
vii
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viii Contents
11 Separation of the Racemic Trans-Stilbene Oxide
by Sub-/Supercritical Fluid Chromatography
Leo Hsu, Genevieve Kennedy, and Gerald Terfloth ...................... 247
12 Chiral Separations Using Macrocyclic Antibiotics
in Capillary Electrophoresis
Timothy J. Ward and Colette M. Rabai ........................................... 255
13 Enantioresolutions by Capillary Electrophoresis
Using Glycopeptide Antibiotics
Salvatore Fanali ................................................................................. 265
14 Separation of Enantiomers by Capillary Electrophoresis
Using Cyclodextrins
Wioleta Maruszak, Martin G. Schmid, Gerald Gübitz,
Elzbieta Ekiert, and Marek Trojanowicz ..................................... 275
15 Chiral Separations by Capillary Electrophoresis
Using Proteins as Chiral Selectors
Jun Haginaka...................................................................................... 291
16 Cellulases as Chiral Selectors in Capillary Electrophoresis
Gunnar Johansson, Roland Isaksson,
and Göran Pettersson ................................................................... 307
17 Use of Chiral Crown Ethers in Capillary Electrophoresis
Martin G. Schmid and Gerald Gübitz .............................................. 317
18 Chiral Separations by Capillary Electrophoresis
Using Cinchona Alkaloid Derivatives as Chiral Counter-Ions
Michael Lämmerhofer and Wolfgang Lindner ............................... 323
19 Chiral Separation by Capillary Electrophoresis
Using Polysaccharides
Hiroyuki Nishi ..................................................................................... 343
20 Chiral Micellar Electrokinetic Chromatography
Koji Otsuka and Shigeru Terabe...................................................... 355
21 Chiral Separation by Capillary Electrophoresis
in Nonaqueous Medium
Marja-Liisa Riekkola and Heli Sirén ................................................ 365
22 Chiral Ligand-Exchange Capillary Electrophoresis
and Capillary Electrochromatography
Martin G. Schmid and Gerald Gübitz .............................................. 375
23 Enantioseparation in Capillary Chromatography and Capillary
Electrochromatography Using Polysaccharide-Type
Chiral Stationary Phases
Bezhan Chankvetadze ....................................................................... 387
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24 Chiral Separation by Capillary Electrochromatography
Using Cyclodextrin Phases
Dorothee Wistuba, Jingwu Kang, and Volker Schurig ................. 401
25 Chiral Separations by Capillary Electrochromatography
Using Molecularly Imprinted Polymers
Peter Spégel, Jakob Nilsson, and Staffan Nilsson ....................... 411
Index ............................................................................................................ 425
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