戴安AS40离子色谱中文操作手册

仪器资料 · 发表于 2017-7-8 15:20:15

戴安AS40离子色谱中文操作手册

1 描述..............................................................................................................................................3
1.1 物理描述............................................................................................................................3
1.1.1 进样装置.................................................................................................................3
1.1.2 控制面板.................................................................................................................4
1.1.3 Sample Out...............................................................................................................8
1.1.4 后面板.....................................................................................................................8
1.2 功能描述............................................................................................................................9
1.2.1 进样装置工作原理.................................................................................................9
1.2.2 排放阀工作原理...................................................................................................13
1.2.3 清洗周期模式.......................................................................................................13
2 操作和维护................................................................................................................................16
2.1 准备样品瓶......................................................................................................................16
2.1.1 清洗瓶子...............................................................................................................16
2.1.2 清洗瓶盖...............................................................................................................16
2.1.3 清洗有过滤头的瓶盖...........................................................................................17
2.1.4 装瓶.......................................................................................................................17
2.2 装载样品瓶架..................................................................................................................18
2.3 选择运行参数..................................................................................................................18
2.4 手动操作..........................................................................................................................18
2.4.1 开始进样...............................................................................................................19
2.4.2 中断操作...............................................................................................................19
2.4.3 跳过样品瓶...........................................................................................................20
2.5 定期维护..........................................................................................................................20
3 故障处理...................................................................................................................................21
3.1 重现性较差......................................................................................................................21
3.2 出现怪异的峰..................................................................................................................21
3.3 没有装样的动作..............................................................................................................22
3.4 进样器停止运行，转为待机状态..................................................................................22
3.5 超高的反压......................................................................................................................23
3.6 样品盒不能前进..............................................................................................................24
3.7 进样器阻塞......................................................................................................................24
3.8 液体泄露..........................................................................................................................25
3.9 气路泄露..........................................................................................................................26
4 维修说明...................................................................................................................................27
4.1 更换接头部件................................................................................................................27
4.1.1 1.55-mm(1/16-in)OD 管路连接说明...................................................................27
4.2 更换进样器接头..............................................................................................................28
4.3 清洗排放阀部件..............................................................................................................29
4.4 清洗损坏的通道面........................................................................................................31
4.5去除排放阀漏气的问题...................................................................................................32
4.6 更换交流电源保险丝......................................................................................................33
1
A 技术指标....................................................................................................................................34
A.1 电学指标：.....................................................................................................................34
A.2 环境指标：.....................................................................................................................34
A.3 物理指标：.....................................................................................................................34
A.4 取样设计：.....................................................................................................................34
A.5 样品瓶.............................................................................................................................35
B 安装说明..................................................................................................................................36
B.1 需要的工具...................................................................................................................36
B.1.1 平台......................................................................................................................36
B.1.2 电源......................................................................................................................36
B.1.3 空气......................................................................................................................36
B.2 安装说明.........................................................................................................................36
B.2.1 样品出口连接......................................................................................................37
B.2.2 气源连接..............................................................................................................37
B.2.3 废液管连接........................................................................................................37
B.3 设置电源开启选项.........................................................................................................38
C AS40默认设置........................................................................................................................39
D AS40继电器控制的设置........................................................................................................41
D.1 继电器控制功能.............................................................................................................41
D.1.1 装样输入继电器..................................................................................................41
D.1.2 Ready 继电器输出控制.......................................................................................42
D 2 装样的时间循环.............................................................................................................43
D.2.1 装样循环的时间顺序..........................................................................................43
D 2.2 润洗运行..............................................................................................................44
D 3 Relay 继电器控制连接的介绍.......................................................................................45