瓦里安气相色谱CP-4900用户手册（英文）

仪器资料 · 发表于 2017-9-3 11:23:57

Table of contents
VARIAN ANALYTICAL INSTRUMENT WARRANTY.................................................................. II
HARDWARE PRODUCTS ............................................................................................................... II
SOFTWARE PRODUCTS................................................................................................................ II
REMEDIES................................................................................................................................... II
LIMITATION OF WARRANTY........................................................................................................... II
LIMITATION OF REMEDIES AND LIABILITY ....................................................................................... II
DECLARATION OF CONFORMITY............................................................................................ III
APPLICABLE STANDARDS............................................................................................................ III
MANUFACTURER - EU................................................................................................................. III
AUTHORIZED REPRESENTATIVE – USA........................................................................................ III
SAFETY INFORMATION............................................................................................................... I
INFORMATION............................................................................................................................... I
OPERATING INSTRUCTIONS ........................................................................................................... I
GENERAL SAFETY PRECAUTIONS ................................................................................................ III
CAUTIONS............................................................................................................................... III
SPARE PARTS AVAILABILITY.........................................................................................................V
SERVICE AVAILABILITY.................................................................................................................V
TABLE OF CONTENTS................................................................................................................ 1
PRE-INSTALLATION REQUIREMENTS ..................................................................................... 2
Environmental requirements................................................................................................. 2
Space requirements.............................................................................................................. 2
Power source........................................................................................................................ 2
Gas supply............................................................................................................................ 3
- External gas supply ................................................................................................. 3
- Safety regards ......................................................................................................... 3
GAS SAMPLES ............................................................................................................................. 3
CP-4900 MICRO-GC INSTALLATION ......................................................................................... 4
INSPECTION ................................................................................................................................ 4
UNPACKING................................................................................................................................. 4
PACKING LIST .............................................................................................................................. 5
CP-4900 Micro-GC ............................................................................................................... 5
Accessories .......................................................................................................................... 6
INSTALLATION.............................................................................................................................. 7
Install Gas Regulators and Set pressures............................................................................ 7
Carrier gas ............................................................................................................................ 7
Connect to Power ................................................................................................................. 7
Connect data handling peripherals....................................................................................... 7
Sample.................................................................................................................................. 8
Heated Sample line .......................................................................................................... 8
Turn power ON ..................................................................................................................... 8
Factory default states and settings....................................................................................... 8
INSTRUMENT OVERVIEW .......................................................................................................... 9
FRONT VIEW................................................................................................................................ 9
BACK VIEW .............................................................................................................................. 10
INSIDE VIEW.............................................................................................................................. 11
CARRIER GAS CONNECTION........................................................................................................ 12
SAMPLE GAS ............................................................................................................................. 13
Handling a sample.............................................................................................................. 13
Unheated Injector Systems ................................................................................... 13
Heated Injector Systems ................................................................................................ 14
HEATED SAMPLE LINE ................................................................................................................ 15
Connect a heated sample line ............................................................................................ 15
POWER..................................................................................................................................... 17
LONG STORAGE PROCEDURE ..................................................................................................... 17
INITIAL OPERATION .................................................................................................................... 18
INITIAL RUN............................................................................................................................... 18
SETTING UP THE TEST METHOD .................................................................................................. 18
INJECTING THE SAMPLE.............................................................................................................. 18
COLUMN CP-SIL 5 CB 6 METER UNHEATED................................................................................ 19
COLUMN CP-SIL 5 CB 4 METER HEATED .................................................................................... 20
COLUMN CP-SIL 5 CB 8 METER HEATED .................................................................................... 21
COLUMN CP SIL13CB TBM 12 METER HEATED ......................................................................... 22
COLUMN HAYESEP 40CM HEATED ............................................................................................. 23
COLUMN MOLSIEVE 5Å 20 METER UNHEATED............................................................................. 24
Conditioning of Molsieve columns ...................................................................................... 24
COLUMN PPQ 10 METER HEATED .............................................................................................. 26
REFERENCE .............................................................................................................................. 27
INSTRUMENT DESCRIPTION ................................................................................................... 27
CARRIER GAS............................................................................................................................ 27
MICRO ELECTRONIC GAS CONTROL (EGC).................................................................................. 28
INJECTOR.................................................................................................................................. 28
COLUMN ................................................................................................................................... 29
DETECTOR................................................................................................................................ 30
TCD..................................................................................................................................... 30
DMD.................................................................................................................................... 30
IN/OUTPUTS............................................................................................................................... 31
EXTERNAL DIGITAL I/O............................................................................................................... 32
Ready/not ready signal....................................................................................................... 32
COMMUNICATION PORTS (COM) ................................................................................................ 33
EXTERNAL ANALOG I/O.............................................................................................................. 34
DIFFERENCE BETWEEN WORKSTATION SOFTWARE PACKAGES.................................................... 35
THE DIFFERENTIAL MOBILITY DETECTOR........................................................................... 36
GENERAL................................................................................................................................ 36
General functionality ........................................................................................................... 36
CP-4900 Micro-GC DMD Channel ..................................................................................... 38
GENERAL OPERATION ................................................................................................................ 39
Tuning the DMD.................................................................................................................. 39
NETWORKING BASICS............................................................................................................. 40
THE NETWORKING MODELS ........................................................................................................ 40
Peer-to-peer........................................................................................................................ 40
Client/Server ....................................................................................................................... 40
Different types of networks ................................................................................................. 40
Star Topology ................................................................................................................. 40
Bus Topology ................................................................................................................. 41
Ring Networks ................................................................................................................ 41
DIFFERENT CABLE TYPES .......................................................................................................... 41
Coaxial............................................................................................................................ 41
Coaxial RG-58................................................................................................................ 42
Twisted Pair.................................................................................................................... 42
PROTOCOLS.............................................................................................................................. 43
Different Types of Protocols: .......................................................................................... 43
The Internet Protocol Suite............................................................................................. 43
IP Addresses .................................................................................................................. 43
The Internet protocol suite.............................................................................................. 43
NETWORKING DEVICES (HUBS, SWITCHES, AND ROUTERS) ......................................................... 44
Hubs and switches are… ............................................................................................... 44
Hubs ............................................................................................................................... 44
Switches ......................................................................................................................... 45
Routers........................................................................................................................... 46
CP-4900 MICRO-GC AND NETWORKS ....................................................................................... 47
Network Requirements of the CP-4900 Micro-GC......................................................... 47
FAQ (FREQUENT ASK QUESTIONS)............................................................................................ 48
GLOSSARY OF NETWORK TERMS ................................................................................................ 49
BNC connector ................................................................................................................... 49
Crossover Cable ................................................................................................................. 49
Domain................................................................................................................................ 49
Ethernet Address ................................................................................................................ 49
Gateway.............................................................................................................................. 49
Host name .......................................................................................................................... 49
Hub ..................................................................................................................................... 49
IP Address .......................................................................................................................... 49
Patch Cable ........................................................................................................................ 50
RJ45 Connector.................................................................................................................. 50
TCP/IP ................................................................................................................................ 50
WORKSTATION SOFTWARE.................................................................................................... 51
CONTROL INSTRUMENT.............................................................................................................. 51
CP-MAITRE ELITE ..................................................................................................................... 52
SERIAL COMMUNICATION ........................................................................................................... 53
ETHERNET COMMUNICATION...................................................................................................... 54
Peer-to-peer: single instrument .......................................................................................... 54
Multiple instrument (local network) ..................................................................................... 55
Global network: Multiple instruments.................................................................................. 56
INSTRUMENT CONFIGURATION ................................................................................................... 57
MODULES CONFIGURATION........................................................................................................ 59
MICRO-GC CONFIGURATION SETUP............................................................................................ 60
COMMUNICATION SETUP............................................................................................................ 61
Serial communication ......................................................................................................... 61
Ethernet communication..................................................................................................... 61
EHTERNET CONNECTION SETUP ................................................................................................. 62
FIND INSTRUMENTS ON THE NETWORK........................................................................................ 63
ASSIGN NEW IP ADDRESS VIA ETHERNET CONNECTION ............................................................... 64
ASSIGN NEW IP ADDRESS VIA SERIAL CONNECTION .................................................................... 65
UPLOAD INSTRUMENT CONFIGURATION ...................................................................................... 66
HARDWARE TAB ........................................................................................................................ 66
USER SETTINGS TAB.................................................................................................................. 68
CP-MAITRE ELITE TAB............................................................................................................... 69
AUTOMATION TAB ...................................................................................................................... 70
VICI VALVE............................................................................................................................... 74
INFO TAB .................................................................................................................................. 75
REMOTE FIRMWARE UPDATE ..................................................................................................... 76
PRESSURE SENSOR CALIBRATION.............................................................................................. 77
RESET MPU-CP-49000............................................................................................................ 77
UPLOAD METHOD...................................................................................................................... 78
DOWNLOAD METHOD................................................................................................................. 78
DOWNLOAD METHOD TAB.......................................................................................................... 78
INSTRUMENT STATUS ................................................................................................................ 79
Extension Box status (optional) .......................................................................................... 80
SHOW AUTOSAMPLER TRAY....................................................................................................... 81
START SINGLE RUN................................................................................................................... 81
EVENT CONFIGURATION............................................................................................................. 82
START SEQUENCE..................................................................................................................... 83
PREVIEW RUN........................................................................................................................... 83
MICRO-GC METHOD SETUP....................................................................................................... 84
CP-4900 TAB ........................................................................................................................... 84
AUX TRACES MAIN TAB.............................................................................................................. 85
TRIGGER TAB............................................................................................................................ 86
COMMON TAB ........................................................................................................................... 87
Stabilization Time ............................................................................................................... 88
ALARM EVENTS TAB .................................................................................................................. 89
Remote control external relays........................................................................................... 90
UserDataStore Address...................................................................................................... 90
Activate Relay if .................................................................................................................. 90
CHANNEL TABS ......................................................................................................................... 92
CHANNEL TAB DMD.................................................................................................................. 95
SAMPLER TAB ........................................................................................................................... 96
AUX TRACES TAB ...................................................................................................................... 97
ELITEEXPORT.DLL USER FILE ..................................................................................................... 98
STANDARD CONTROL .............................................................................................................. 100
EXTERNAL STARTED................................................................................................................ 100
AUTO SAMPLER CONTROL ....................................................................................................... 101
ALARM SETUP (CONTACT CLOSURES) ....................................................................................... 101
External Pump Control...................................................................................................... 102
ACQUIRE EXTERNAL ANALOG SIGNALS..................................................................................... 102
EXTERNAL DEVICE SYNCHRONIZATION...................................................................................... 103
CP-4900 AND SAMPLER EXTERNAL STARTED........................................................................... 103
REMOTE ACCESS INSTRUMENT STATUS ................................................................................... 104
GENERAL ERROR STATE.......................................................................................................... 106
VARIAN USERLINK APPLICATIONS ............................................................................................. 108
CP-4900 External Relays ................................................................................................. 108
CP-4900 instrument status including analog inputs ......................................................... 109
UserDataStore addresses of Varian userlink applications ............................................... 109
EXTERNAL DEVICES ................................................................................................................. 111
CYCLE WITH STATIC (ELECTRONIC) PRESSURE.............................................................. 113
CYCLE WITH ELECTRONIC PRESSURE CONTROL............................................................ 114
COLUMN MODULE CONDITIONING ...................................................................................... 115
BACKFLUSH OPTION ............................................................................................................. 116
Description........................................................................................................................ 117
Tuning............................................................................................................................... 118
SHIPPING INSTRUCTIONS ..................................................................................................... 119
CLEANING INSTRUCTIONS.................................................................................................... 119
DISPOSAL INSTRUCTIONS.................................................................................................... 119
ERROR LIST............................................................................................................................. 120