岛津CLASS-VP_Ver.6常见问题解答

仪器资料 · 发表于 2018-2-8 13:42:45

索引
1. 安装·············································································································1
问题 1.1. 现有LC-10A Series 单元可以通过 CLASS-VP 控制？·······························1
问题 1.2. 哪些 LC-VP Series 版本号与 CLASS-VP 兼容？········································1
问题 1.3. 哪些 SPD-M10Avp 版本号与 CLASS-VP 兼容？········································1
问题 1.4. CLASS-VP 可以在 Windows NT 下运行吗？···············································1
问题 1.5. 使用软件狗时，CLASS-VP 有时根本不启动或者过了很长时间以后才启
动，这是否说明计算机有问题？·····································································1
问题 1.6. 我的计算机不能与SCL-10Avp（或 LC-2010）正确连接，这可能是什
么原因造成的？································································································1
问题 1.7. 我的计算机偶尔会由于RS-232C 通信错误而死机，有好的对策吗？········1
问题 1.8. 使用 CLASS-VP 控制多个 LC 系统时，SCL-10Avp 和 LC-2010 可以
连接到从市面上买到的任何 RS-232C 插板上吗？·······································2
问题 1.9. 尽管 PDA 检测器已连接到计算机上，但 CLASS-VP 仍无法识别此单
元。···················································································································2
问题 1.10. 在通过SCSI 接口连接 SCL-10Avp 后，此仪器不工作，出了什么问
题？···················································································································2
问题 1.11. 我想在SCL-10Avp 上安装 PC-55N 双通道插板，该怎样设置 DIP 开
关（双列直插式开关）？················································································2
问题 1.12. 我使用的是 PDA 检测器和 Windows NT，然而“PDA Calibration”程序
却无法使用。····································································································3
问题 1.13. 请解释一下如何重新安装CLASS-VP。还有，升级 CLASS-VP 时，是
否有专用的升级磁盘？····················································································3
问题 1.14. 尽管已安装了软件狗，但在打开 CLASS-VP Instrument 窗口时，仍显示
“This file can not be opened in demo mode”这一警告消息。·······················3
问题 1.15. 如果管理员忘记了CLASS-VP 的登录口令，那么初始化 System
Administration 设置的步骤是什么？·······························································3
问题 1.16. 我更换了 LC 单元耗材，该如何重新设置系统检测参数？·························3
问题 1.17. 我更换了PDA 检测器光源，该如何重新设置光源的运行时间？···············4
问题 1.18. 启动 PDA Calibration 时，显示出“Unable to load PdaVp16.dll”这一消
息，出了什么问题？························································································4
问题 1.19. 在一台计算机上可以同时使用CLASS-VP 5.xx 版和 6.0 版吗？···············4
2. 配置·············································································································5
问题 2.1. AutoConfig 可以用来检测和配置 PDA 检测器吗？·····································5
问题 2.2. 检测器Configuration 字段中的 Base Period 的意思是什么？在此应输
入什么值？·······································································································5
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问题 2.3. 尽管可用于 2mL 进样的选配定量管已连接到 LC-2010 自动采样器
上，但不能在 CLASS-VP 软件中将 Injection Volume 值设为大于
100uL。为什么？·····························································································5
问题 2.4. Recycling Valve 可以由 CLASS-VP 6.0 版控制吗？····································5
3. 方法·············································································································6
问题 3.1. 峰处理参数在哪里设置？················································································6
问题 3.2. 峰处理参数的最小面积是如何计算的？·························································6
问题 3.3. 如果在Integration Events Table 的多行中指定了具有相同时间的相同命
令，那么将使用哪一条命令？·········································································6
问题 3.4. [Method] > [Instrument Setup] 菜单的 <System Controller> 选项框中显示
的 Trigger Type 是什么意思？·······································································6
问题 3.5. 在哪里设置 Fraction Collector（馏份收集器）程序？···································6
问题 3.6. 馏份收集器程序有模拟功能吗？·····································································7
问题 3.7. 梯度曲线和馏份收集器程序有图形化设置功能吗？······································7
问题 3.8. 校准曲线类型及其加权方法可以在 Peak 表中选择。也可以在 [Method]
> [Review Calibration Curve] 中选择这些项。两者之间有什么不同？·········7
问题 3.9. Peak 表中有 10 个浓度级别的列。然而极少情况下这 10 个级别都使
用，并且由于存在此 10 列，所以查看该表很困难。··································7
问题 3.10. 如何将数据传输到 EXCEL 中？····································································7
问题 3.11. 如何更改理论塔板数和分离度计算方法？·····················································7
问题 3.12. 我希望自动将数据复制到网络服务器，如何做到这一点？··························7
问题 3.13. 如何进行数据背景补偿？················································································8
问题 3.14. 如何设置 System Suitability（系统适应性）？··············································8
问题 3.15. 可以将 Calibration Curve 的竖轴指定为 Amount 吗？································8
问题 3.16. 请解释一下如何设置和使用方法的Audit Trail（审计跟踪）。···················8
问题 3.17. 一旦激活一个方法的审计跟踪，就再也不能停用，这样很不方便。··········8
问题 3.18. 请解释一下如何将数据转换成 AIA 格式，以及如何导入 AIA 格式的
数据。···············································································································9
问题 3.19. 峰保留时间和面积无法正确传输，这是否因为某些设置不正确？···············9
问题 3.20. 在[Method] > [PDA Setup] 的 General 选项框中设置 Run Time、
Wavelength Range 和 Sampling Period 时出现错误。请解释一下这些参
数之间的关系。································································································9
问题 3.21. 请解释一下[Method] > [PDA Setup] 的 General 选项框中的 Sampling
Frequency (Period) 和 Time Constant 之间的区别。·····································9
问题 3.22. 在[PDA Setup] 的 <Multi-Chromatogram> 选项框中改变了波长和带宽
时，Peak 表中的分析通道将变为另一通道。为什么会出现这种情况？······10
问题 3.23. 峰可以用光谱的 Similarity 标识吗？·····························································10
问题 3.24. 在 [Method] > [Peak/Group Table] 菜单中有一个 Calib Flag 列。此列的
选项有 Average 和 Replace。另外，序列表的 Run Type 列中还有一个
Average Replicates 选项。请解释一下这些项之间的联系。·························10
问题 3.25. 请解释一下如何通过相对保留时间设置已命名的峰。··································12
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4. 自动进样器程序···························································································13
问题 4.1. 如何编辑预处理程序？····················································································13
问题 4.2. 自动进样器程序设置窗口包含 Dilution 和 Reagent 选项。这些功能可
在 SIL-10A 或 SIL-10AXL 中使用吗？在 SCL-10Avp 上，这些功能好
像只能用于 SIL-10ADvp。·············································································13
问题 4.3. 对建立自动进样器预处理程序有什么限制吗？··············································13
5. 分析·············································································································14
问题 5.1. 每次启动软件时都要登录有点太麻烦。请解释一下如何禁用登录功能。···14
问题 5.2. 如何执行斜率测试？························································································14
问题 5.3. 使用色谱图屏幕的弹出菜单的[Graphical Programming] 菜单项中的
[SLOPE] 执行斜率测试时，有时会出现“Not enough points for SLOPE
calculation. Please select a longer time interval.”这一消息。应如何确定时
间周期？···········································································································14
问题 5.4. 请解释一下开始运行前应如何监视基线。·····················································14
问题 5.5. 当用手动进样器注入样品时，SCL-10Avp 开始执行 Run。然而，
CLASS-VP 只显示一个要求开始采集数据的信息框，但并不执行采集。···14
问题 5.6. 我的系统中有一个二极管阵列检测器 (SPD-M10Avp)。当触发器类型设
为 External 并执行 Run 时，SCL-10Avp 执行 Run，但 CLASS-VP 并
不开始采集数据。而当触发器类型设为 Manual 时，没有任何问题。·······15
问题 5.7. 可以显示梯度曲线吗？····················································································15
问题 5.8. 执行 Run 时，如果已存在一个同名的数据文件，将会显示一条错误消
息而且 Run 不启动。应如何覆盖数据文件？···············································15
问题 5.9. 即使 USP Width 已指定为一个色谱图注释项，但在注释字段中只显示
为 0。另外，USP Width 的切线则无法显示。·············································15
问题 5.10. 尽管二极管阵列检测器 (SPD-M10Avp) 工作正常，但无法通过 direct
control（直接控制）来打开和关闭光源。······················································15
问题 5.11. 显示 PDA 等高线图时，需要很长时间才显示出绘制的图形。···················15
问题 5.12. 在 PDA Mixed View 中，用鼠标右键单击光谱屏幕以显示弹出菜单，但
无法使用 Operation 或 Calc Lambda-max.. 菜单项。··································16
问题 5.13. 在 PDA Mixed View 中，如何向 Similarity 表中添加光谱图？ ·················16
问题 5.14. 在 PDA Mixed View 中，纯度曲线和峰轮廓图无法显示。·························16
问题 5.15. 在 PDA Mixed View 中，如何从色谱图窗格中选择光谱或从光谱窗格中
选择波长？·······································································································16
问题 5.16. 尽管 SCL-10Avp 状态已变为“Run”，CLASS-VP 还是不启动数据采
集。···················································································································16
问题 5.17. 按下 [Preview] 按钮时，显示出“All channels are off. No acquisition will
be performed”这一消息，出现了什么错误？················································16
问题 5.18. 如何改变数据图的 Y 轴标尺？······································································16
6. 序列·············································································································17
问题 6.1. 编辑一个序列时，我希望让数据文件名自动递增，比如“TEST01”、
“TEST02”... 如何做到这一点？····································································17
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问题 6.2. 我使用 [File] > [Sequence] > [New] 命令创建了下面这样一个表： Data
file: TEST Start vial number: 0 End vial number: 0 Repetitions per run:
2 当执行 Sequence Run 时，数据文件将以什么名称保存？····················17
问题 6.3. 使用 [File] > [Sequence] > [New] 命令进行了下面的设置： Data file:
TEST Start vial number: 0 End vial number: 0 Repetitions per run: 2
选中“Repetitions create multiple records.”复选框。在这种情况下，
表的数据文件名会是什么？·············································································17
问题 6.4. 编辑一个序列时，Clear All Calibration 和 Clear Calibration at Level 这两
种运行类型之间的区别是什么？·····································································17
问题 6.5. 分类校准的 Standard、Std /w Clear Calib 和 Sequence 之间有什么区别？··18
问题 6.6. 执行样品序列时，未生成摘要报告，应如何设置？······································19
问题 6.7. 即使在使用 UV 检测器的双波长模式或使用 PDA 检测器的多谱图数
据时，也可以创建摘要报告吗？·····································································19
问题 6.8. 执行一个样品序列时，未创建此序列的校准报告，应如何设置它？···········19
问题 6.9. 执行一个样品序列时，未创建此序列的 Duplicate（平行）报告，应如何
设置它？···········································································································19
问题 6.10. 执行一个样品序列时，未创建此序列的 Spike（回收率）报告，应如何
设置它？···········································································································20
问题 6.11. 执行一个样品序列时，未创建此序列的 Check Std（控制样）报告，应
如何设置它？····································································································20
问题 6.12. 执行一个样品序列时，未创建此序列的 System Suitability（系统适应
性）报告，应如何设置它？·············································································20
问题 6.13. 如何在序列 Run Type 列表中使用 Shut Down (SHD) 选项？·····················20
问题 6.14. 如何使用 Action 设置的 Test 组合框中的 Hardware Status 选项？··········21
问题 6.15. 如果所有要同时测量的组分未包含在一个标准溶液中，则应如何设置
Peak 表和序列？······························································································21
问题 6.16. 当在一个序列的 Action 功能中指定 Reinject 时，没有地方可输入新的
数据文件名。执行此功能时，原有数据会被覆盖吗？··································21
问题 6.17. 尽管在一个序列中已选择了 Bracketing 模式，标样数据仍未用作校准数
据。···················································································································21
问题 6.18. 推荐哪一版本的 MS-EXCEL 用于 Sequence Wizard？································21
7. 报告·············································································································23
问题 7.1. 执行 Run 时，未创建报告。应如何设置方法报告？···································23
问题 7.2. [Method] > [Custom Report] 与 [Sequence] > [Custom Report] 之间有何区
别？···················································································································23
问题 7.3. 可以将梯度曲线输出到报告中吗？···································································23
问题 7.4. 指定 PDA 多色谱图通道时，如何查看标准报告，如 Area% 报告？········23
问题 7.5. 输出报告时，有时会出现 BDL。这说明什么问题？····································23
问题 7.6. 当方法的 [Custom Report] 中包括 Library Search Results 时，只打印出
表的标题。·······································································································23
问题 7.7. 色谱图和表可以并排打印吗？········································································24
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问题 7.8. 两个图形（如色谱图）可以用完全相同的格式打印并横向排列吗？···········24
问题 7.9. 菜单项 [File] > [Report Template] > [Open] 为灰色，所以无法打开报告
模板。···············································································································24
问题 7.10. 如何删除已插入到 Custom Report 中的图形（如校准曲线）？··················24
问题 7.11. 选择 [Report] > [View / Print]) > [Sequence Custom Report] 时不显示报
告。···················································································································24
问题 7.12. 如何在 Custom Report 中插入分页符？·························································24
问题 7.13. 报告模板文件有三种扩展名：REP、SRP 和 BRP。它们有何区别？·········25
问题 7.14. 当在 [Method] > [PDA Setup] 的 <Multi-chromatogram> 选项框中改变
了通道波长和（或）带宽时，报告中不打印色谱图。··································25
问题 7.15. 当色谱图图形显示在 Custom Report 中时，图形轴上的值和峰注释中的
字符不可读，即使改变字体，也还是一样。··················································25
问题 7.16. Similarity Index 值在 Custom Report 中变成了 0，应该怎样设置它？········25
问题 7.17. 如何初始化 Custom Report（定制报告）设置？···········································25
问题 7.18. 如何将Run Report（运行报告）变成十进制数？·········································25
8. POST RUN 分析··························································································26
问题 8.1. 在 Offline Processing 和 Instrument 1 to 4 窗口中都可以执行Post Run
分析。这之间有什么区别？·············································································26
问题 8.2. 我在 Offline Processing 窗口中选择 Instrument 1 to 4。那么当我选择
[File] > [Data] > [Open] 并选中 Open With Method 时，仪器的方法也会
改变吗？···········································································································26
问题 8.3. 是否有一种 Chromatopac Integration Events 的手动处理功能？···················26
问题 8.4. 如何对两个色谱图相减得到的新色谱图进行分析？······································26
9. 其他项·········································································································27
问题 9.1. CLASS-LC10 的色谱图文件可以直接读入 CLASS-VP。在 CLASSLC10
中应如何读取 CLASS-VP 色谱图数据？············································27
问题 9.2. 可以对用 CLASS-VP 采集到的数据进行 GPC 计算吗？ ···························27
问题 9.3. 仪器、方法和数据名称显示在标题栏内。在方法名旁边，有时会显示
Read-only。为什么？ ·······················································································27
问题 9.4. 在 <System Administration> 菜单中选择 Purchased Options 时，将显示
产品系列号，这说明什么问题？·····································································27
问题 9.5. 我希望在 Run 期间直接向 MO 或可拆卸的磁盘中写入数据。·················27
问题 9.6. 绘制等高线图和三维谱图过程中可以取消绘制吗？······································27
问题 9.7. 怎样才能删除 Instrument Activity Log？························································28
问题 9.8. 从 Spectrum 窗口的弹出菜单中选择 [Library Search] > [Use Method
Parameter] 时，未执行 Library Search（谱库搜索）。·································28
问题 9.9. 怎样才能将色谱图和光谱图形粘贴到 Microsoft Word 中？························28
问题 9.10. 怎样才能将等高线图和 3D 图形粘贴到 Microsoft Word 中？····················28