ICP-MSAgilent形态分析技术手册第二版

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Introduction to Hyphenated ICP-MS 5
HPLC-ICP-MS 9
Introduction to HPLC-ICP-MS 10
Speciation of Gaseous Arsines using Chemotrapping followed by HPLC-ICP-MS 11
Determination of Inorganic Arsenic in Rice by Anion Exchange HPLC-ICP-MS 13
Arsenic Speciation in Rice — A Routine HPLC-ICP-MS Method? 15
Determination of Arsenic Species in Marine Samples using Cation Exchange HPLC-ICP-MS 17
Application of Compound Independent Calibration Software to Arsenic Speciation 20
Benefits of HPLC-ICP-MS Coupling for Mercury Speciation in Food 23
Mercury Speciation Measurements in Fish Tissues and Sediments by HPLC-ICP-MS 26
Determination of Mercury Species in Crude Oil by Speciated Isotope Dilution LC-ICP-MS 29
Low-Level Speciated Analysis of Cr(III) and Cr(VI) using LC(IC)-ICP-MS 32
Determination of Hexavalent Chromium in NIST SRM 2701 by Speciated Isotope Dilution Mass 36
Spectrometry (EPA Method 6800) using IC-ICP-MS
HPLC-ICP-MS for Preliminary Identification and Determination of Methyl-Selenium Metabolites of 39
Relevance to Health in Pharmaceutical Supplements
Selenium Speciation Analysis by LC-ICP-MS with Mass Balance Calculations for Se-Enriched Yeasts 42
Antimony Speciation in Natural Waters by HPLC-ICP-MS 44
Measurement of Total Antimony and Antimony Species in Mine Contaminated Soils by ICP-MS and 46
HPLC-ICP-MS New Hyphenated Instrumental Combination for Speciation — Solid-Phase Microextraction (SPME) 48
Coupled to
HPLC-ICP-MS
Treble Detection of Heteroatom-Tagged Green Fluorescence Protein by HPLC Photodiode Array (PDA) 51
Detector, Fluorescence Detector (FD) and ICP-MS
Determination of Ceruloplasmin in Human Serum by Immunoaffinity Chromatography and Size- 54
Exclusion Chromatography (SEC) ICP-MS
Application of ICP-MS to the Analysis of Phospholipids 57
Analysis of Glyphosate, Gluphosinate, and AMPA by Ion-Pairing LC-ICP-MS 60
Troubleshooting LC-ICP-MS Systems 62
GC-ICP-MS 65
Introduction to GC-ICP-MS 66
Analysis of Polybrominated Diphenyl Ether (PBDE) Flame Retardants by GC-ICP-MS 68
Analysis of Sulfur in Low-Sulfur Gasoline by GC-ICP-MS 70
Characterization of Metalloporphyrins in Crude Oils by High Temperature Simulated Distillation using 72
GC-ICP-MS Determination of Mercury Species in Whole Blood by Calibration Curve-Free Speciated Isotope 75
Dilution Solid-Phase Microextraction (SPME) GC-ICP-MS with Microwave Assisted Isotope
Equilibration and Extraction
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Determination of Phosphoric Acid Triesters in Human Plasma using Solid-Phase Microextraction 77
(SPME) and GC-ICP-MS
Determination of Arsine in Ethylene and Propylene by GC-ICP-MS 80
Determination of Organotin Compounds in Urine Samples using GC-ICP-MS 82
Specific Migration of Organotin Compounds from Food Contact Materials — Selective Determination 85
by GC-ICP-MS
Troubleshooting GC-ICP-MS Systems 89
Multi-MS 91
Introduction to Multi-MS — Coupling HPLC with Elemental and Molecular Mass Spectrometry 92
Mercury Speciation in Rice — More Than Methylmercury using HPLC-ICP-MS/Electrospray 93
Ionization (ESI) MS
Speciation of Selenometabolites in the Liver of Sea Turtles using HPLC-ICP-MS and Electrospray 95
Ionization (ESI) MS-MS
Determination and Quantification of Non-Metal Bound Phytochelatins by HPLC-ICP-MS/Electrospray 98
Ionization (ESI) MS
Fractionation and Identification of Arseno Fatty Acids from Cod-Liver Oil by the Parallel Use of HPLC 100
On-Line with ICP-MS and Electrospray Ionization (ESI) MS
Selenium Speciation in Soybean using HPLC-ICP-MS and Electrospray Ionization (ESI) Ion Trap (IT) 102
MS
Multi-Elemental Exposure of Freshwater Plants and Identification of Heteronuclear Phytochelatin 105
Complexes by HPLC Electrospray Ionization (ESI) MS/ICP-MS
Protein Phosphorylations as Potential Biomarkers in Cerebral Spinal Fluid 109
Field-Flow Fractionation (FFF) ICP-MS 111
Introduction to Field-Flow Fractionation (FFF) ICP-MS 112
Investigation of the Relationship between Salinity and the Adsorption of Different Elements on the 114
Surface of Nanoparticles in Natural Water Samples
Quantitative Characterization of Gold Nanoparticles by Field-Flow Fractionation (FFF) Coupled 117
On-Line with Light Scattering Detection and ICP-MS
Asymmetric Flow Field-Flow Fractionation (AF4) ICP-MS for Speciation of Various Elements in 119
Aggregated Proteins
Other Speciation Techniques 123
Introduction to ‘Other’ Speciation Techniques 124
Absolute Quantification of a Metalloprotein using Species-Specific Isotope Dilution Methodology 125
and Gel Electrophoresis (GE) Laser Ablation (LA) ICP-MS
Contribution of Capillary Electrophoresis (CE) ICP-MS to Metalloprotein Analysis 127
Determination of Roxarsone and its Transformation Products using Capillary Electrophoresis (CE) 129
Coupled to ICP-MS
Acknowledgements 132
Index 133