PROCEDURES FOR OPERATION OF THE JEOL 6330F FIELD EMISSION SEM

仪器资料 · 发表于 2018-7-2 17:01:06

PROCEDURES FOR OPERATION OF THE JEOL 6330F FIELD EMISSION SEM

Getting Started
When you approach the microscope, the pumps and water supply should be running
smoothly.
Turn on the electronics using the button marked I under the bench.
Turn on the monitor. If the ‘states’ page is shown with an orange highlighted box, there
has been a failure, call the Technician.
This microscope is kept at ultra high vacuum status so it is vital that the holders are kept
clean, sample stubs are ALWAYS handled wearing gloves, and that samples are
completely dry before they are put into the machine.
GLOVES SHOULD ALWAYS BE USED WHEN LOADING THE SAMPLES INTO THE
MICROSCOPE.
Please be very gentle with the microscope – do not force the airlock door or sample rod.
Also do not continually change kV or WD as the microscope takes a little time to settle
after any big changes.

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