ARL3460用户手册（英文）

仪器资料 · 发表于 2018-7-1 15:47:21

ARL3460用户手册（英文）

1 INTRODUCTION..................................................................................... 1-1
INTRODUCTION......................................................................................................1-1
Convention...........................................................................................................1-1
WINOE SOFTWARE DOCUMENTATION...............................................................1-2
Summary of Operator Manual..............................................................................1-2
SOFTWARE INSTALLATION ..................................................................................1-4
Installing Documentation Options from CD-ROM ................................................1-5
Forewords........................................................................................................1-5
Starting Installation Program............................................................................1-5
Installing the Acrobat Reader Option ...............................................................1-6
Installing Documentation Manuals ...................................................................1-7
Viewing or Printing Documentation ....................................................................1-10
LOGGING INTO WINOE SOFTWARE ..................................................................1-12
INSTRUMENT INITIALISATION ............................................................................1-16
USER INTERFACE STRUCTURE.........................................................................1-17
Display and Modes.............................................................................................1-17
Icons of the Functions Frame ............................................................................1-20
Home .............................................................................................................1-21
Layout ............................................................................................................1-21
Log Off ...........................................................................................................1-21
Exit.................................................................................................................1-21
About .............................................................................................................1-22
WORKING WITH SHORTCUTS............................................................................1-23
2 UNKNOWN SAMPLE ANALYSIS .......................................................... 2-1
INTRODUCTION......................................................................................................2-1
UNKNOWN SAMPLES ANALYSES AND MEASUREMENTS.................................2-2
Analysing Concentrations in Unknown Samples..................................................2-2
Starting Analysis Process with Shortcut...........................................................2-3
Starting Analysis Process with Generic Icon....................................................2-5
Amending Buttons Before Analysis..................................................................2-7
Changing Task ...................................................................................................................... 2-7
Selecting Program................................................................................................................. 2-8
Assigning Bad Sample .......................................................................................................... 2-9
Analysis Runs ..................................................................................................2-9
Colours and Result Flags.................................................................................................... 2-15
Ending Analysis Process ...............................................................................2-16
Results Processing Options...........................................................................2-17
Modify.................................................................................................................................. 2-18
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Table of Content
II WinOE Operator Manual AA83496
Store.................................................................................................................................... 2-18
Transmit .............................................................................................................................. 2-19
Quality Check...................................................................................................................... 2-19
Quality Sort.......................................................................................................................... 2-19
Charge Correction............................................................................................................... 2-19
Send to SPC ....................................................................................................................... 2-20
Analysing Intensities in Unknown Samples........................................................2-20
PROCESS WITH SELECTED FEATURES ...........................................................2-22
Analyses with Type Standard Correction ...........................................................2-22
Analyses with Quality Check..............................................................................2-24
Analyses with Quality Sort .................................................................................2-26
Analyses with Charge Correction .......................................................................2-28
Analyses with Manual Inputs..............................................................................2-28
Results Modification...........................................................................................2-29
Bad Sample Transmission .................................................................................2-29
BEHAVIOUR WITH SELECTED MODES..............................................................2-30
Analysis Averaging.............................................................................................2-30
Bad Runs ...........................................................................................................2-33
Pre-Defined Sample Mode.................................................................................2-34
Print Mode..........................................................................................................2-35
Storage Mode ....................................................................................................2-35
Transmit Mode ...................................................................................................2-36
SPC Transfer .....................................................................................................2-36
SPC Bad Sample Transmission ....................................................................2-37
Display Mode .....................................................................................................2-37
3 CONTROL SAMPLE ANALYSIS............................................................ 3-1
ANALYSING CONTROL SAMPLES ........................................................................3-2
Starting Control Sample Analysis Process with Shortcut .....................................3-3
Starting Control Sample Analysis Process with Generic Icon ..............................3-5
Analysis Runs ......................................................................................................3-9
Ending Analysis Process....................................................................................3-10
TRANSFER TO SPC..............................................................................................3-11
Bad Sample Transmission .................................................................................3-11
SPC Messages ..................................................................................................3-11
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Table of Content
AA83496 WinOE Operator Manual III
4 STANDARDISATION UPDATE .............................................................. 4-1
RUNNING THE STANDARDISATION UPDATE TASK ...........................................4-2
Starting Standardisation Update Process with Shortcut.......................................4-3
Starting Standardisation Update Process with Generic Icon................................4-5
Analysis Runs ....................................................................................................4-10
Ending Analysis Process....................................................................................4-11
Reproducibility Check ........................................................................................4-13
REPLACE SETTING-UP SAMPLES......................................................................4-14
Procedure ..........................................................................................................4-14
LASER POWER DRIFT UPDATE..........................................................................4-15
5 TYPE STANDARDISATION UPDATE.................................................... 5-1
INTRODUCTION......................................................................................................5-1
RUNNING THE TYPE STANDARD UPDATE TASK ...............................................5-2
Starting Type Standard Update Process with Shortcut........................................5-3
Starting Type Standard Update Process with Generic Icon .................................5-5
Analysis Runs ......................................................................................................5-8
Ending Analysis Process......................................................................................5-9
6 INSTRUMENT STATUS AND PROFILE ................................................ 6-1
INSTRUMENT STATUS...........................................................................................6-1
Read Instrument Status .......................................................................................6-2
PROFILE..................................................................................................................6-4
Direct Profile ........................................................................................................6-5
Direct Profile Configuration ..............................................................................6-5
Monitoring Options...........................................................................................6-6
Running Direct Profile......................................................................................6-8
Integrated Profile................................................................................................6-11
Integrated Profile Configuration .....................................................................6-11
Running Integrated Profile .............................................................................6-12
Graphical Monitoring......................................................................................6-15
7 RETRIEVE RESULTS AND STATISTICS .............................................. 7-1
INTRODUCTION......................................................................................................7-1
RESULTS RETRIEVAL............................................................................................7-2
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Table of Content
IV WinOE Operator Manual AA83496
Starting Result Retrieval Process with Generic Icon............................................7-2
Starting Result Retrieval Process with Shortcut...................................................7-3
Selection Criteria for Results Retrieval ................................................................7-4
Procedure for Results Retrieval ...........................................................................7-4
Database Selection..........................................................................................7-5
Task Selection .................................................................................................7-5
Analytical Program Selection ...........................................................................7-6
Sample Identity Filters .....................................................................................7-7
Time Period Filters...........................................................................................7-7
Result Type Filters...........................................................................................7-8
Terminating Selections ....................................................................................7-9
Handling on Retrieved Results.............................................................................7-9
Action Buttons....................................................................................................7-10
Actions Summary...........................................................................................7-10
Modifying Sample ..........................................................................................7-12
Export Results ...............................................................................................7-13
Transmission Options ....................................................................................7-16
Statistics ........................................................................................................7-17
Quality Check ................................................................................................7-19
Quality Sort ....................................................................................................7-21
Charge Correction..........................................................................................7-22
Transfer to SPC .............................................................................................7-22
8 USING CHARGE CORRECTION OPTION............................................. 8-1
PERFORMING CHARGE CORRECTION ANALYSES............................................8-2
Using Quality Check.............................................................................................8-4
Using Quality Sort ................................................................................................8-5
Using Retrieved Results.......................................................................................8-6
DESCRIPTION OF CHARGE CORRECTION .........................................................8-7
Normal Situation ..................................................................................................8-8
Special Situations ..............................................................................................8-10
Charge Correction with Automation ...................................................................8-12
CHARGE CORRECTION EXAMPLE.....................................................................8-13
Analysis with Quality Check ...............................................................................8-13
Charge Correction without Dilution ....................................................................8-13
Charge Correction with Dilution .........................................................................8-14
9 USING AUTOMATION MODE OPTION ................................................. 9-1
SETTING AUTOMATIC MODE................................................................................9-1
USING WINOE IN AUTOMATIC MODE ..................................................................9-4
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Table of Content
AA83496 WinOE Operator Manual V
10 USING REMOTE SAMPLE DEFINITION MODE OPTION................ 10-1
SETTING REMOTE SAMPLE DEFINITION MODE...............................................10-1
USING WINOE IN REMOTE SAMPLE DEFINITION MODE .................................10-5
11 USING METAVERAGE OPTION ...................................................... 11-1
MANUAL OPERATION ON METAVERAGE PROCESS .......................................11-1
Quality Control of the Metaverage .....................................................................11-5
BEHAVIOUR WITH AUTOMATED MODES ..........................................................11-6
Metaverage with Automatic Mode......................................................................11-6
Metaverage with Remote Sample Definition Mode ............................................11-6
12 USING ANALYSIS RECALCULATION OPTION .............................. 12-1
INITIATING ANALYSIS RECALCULATION...........................................................12-2
Changing Sample Signature ..............................................................................12-4
Redefining Sample Analysis Environment .........................................................12-5
Recalculation Process........................................................................................12-6
RULES AND TRACING..........................................................................................12-8
Results Retrieval ................................................................................................12-8
Transmission to SPC .........................................................................................12-9
Other Transmission............................................................................................12-9
A ALARMS LIST........................................................................................A-1
ICS ALARMS LIST.................................................................................................. A-1
ALARM SEVERITY ............................................................................................... A-12
B ALARM REPORT MONITOR..................................................................B-1
C KEYBOARD OPERATIONS ...................................................................C-1
D WINOE ICONS .......................................................................................D-1
ICON COMPOSITION AND COLOURS.................................................................. D-1
Colours meaning.................................................................................................D-2
Polygons meaning...............................................................................................D-2
Elements meaning ..............................................................................................D-3
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Table of Content
VI WinOE Operator Manual AA83496
Other symbols..................................................................................................... D-4
ALL WINOE ICONS AND SHORT-CUTS ............................................................... D-5
Icons ................................................................................................................... D-5
Menu Functions Frame and Log-In.................................................................D-5
Generic Icons..................................................................................................D-5
Instrument Icons ............................................................................................. D-6
General Icons .................................................................................................D-7
Analysis Tasks Icons .................................................................................... D-10
Instrumental Check Icons ............................................................................. D-11
Check Tasks Icons ....................................................................................... D-12
Short-Cuts and Desktop Icons ..........................................................................D-13
INDEX .............................................................................................................I