TABLE OF CONTENTS
BEFORE USING THIS PYROLYZER A-2
PRODUCT WARRANTY A-2
FOR YOUR SAFETY A-3
IMPORTANT NOTE WHEN OPERATING PYROLYZER OVER 800°C A-3
CONTENTS IN THE PACKAGE A-4
TABLE OF CONTENTS A-5
CHAPTER 1 ABOUT MULTI-SHOT PYROLYZER 1-1
1.1 BACKGROUND OF DEVELOPMENT 1-1
1.2 FEATURES OF EGA/PY-3030D 1-3
1.3 PERIPHEREAL DEVICES 1-4
1.4 SCHEMATIC OF MULTI-SHOT PYROLYZER FURNACE 1-5
CHAPTER 2 SPECIFICATIONS 2-1
2.1 SPECIFICATIONS 2-1
CHAPTER 3 INSTALLATION 3-1
3.1 PREPARING INSTALLATION 3-1
3.1.1 Before installation 3-1
3.1.2 Pumping down MS (for saving installation time) 3-2
3.2 REPIPING CARRIER GAS LINE 3-3
3.3 SETTING UP GC INJECTION PORT 3-4
3.3.1 Replacing septum nut of GC injection port 3-4
3.3.2 Replacing septum and applying release agent 3-4
3.3.3 About injection port liner 3-4
3.4 SETTING UP PYROLYZER FURNACE 3-4
3.4.1 Installing quartz pyrolysis tube to pyrolyzer 3-4
3.4.2 Attaching interface union and needle 3-4
3.4.3 Mounting pyrolyzer on GC 3-5
3.5 CONNECTING TEMPERATURE CONTROLLER 3-5
3.5.1 Connecting power cable to outlet 3-5
3.5.2 Connecting to control PC 3-5
3.5.3 Hooking up remote signal cable 3-5
3.6 CONNECTING COOLING GAS LINE 3-5
3.6.1 About cooling gas 3-5
3.6.2 Connecting temperature controller and pyrolyzer 3-6
3.6.3 Connecting aquarium air pump 3-7
3.7 INSTALLING PERIPHERAL DEVICES 3-8
3.7.1 Connecting Auto-Shot sampler (AS-1020E) 3-8
3.7.2 Connecting other peripheral devices 3-8
A-5
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3.8 INSTALLING CONTROL SOFTWARE 3-9
3.8.1 Installing USB serial communication device driver 3-9
3.8.2 Installing control software 3-10
3.8.3 Setting COM port 3-10
3.9 FRONT, BACK, SIDE, AND TOP VIEWS 3-12
3.9.1 Pyrolyzer 3-12
3.9.2 Temperature Controller 3-13
CHAPTER 4 USING CONTROL SOFTWARE 4-1
4.1 START UP AND SCREEN LAYOUT 4-1
4.1.1 Starting program 4-1
4.1.2 Screen layout 4-2
4.2 BEFORE STARTING AN ANALYSIS 4-4
4.2.1 System configuration 4-4
4.2.1.1 Selecting a device or devices 4-4
4.2.1.2 Abbreviations for accessory devices 4-4
4.2.1.3 Using air as atmosphere gas 4-4
4.2.2 Set-up interface temperature 4-6
4.3 SET-UP ANALYTICAL MODES AND OPERATION 4-7
4.3.1 Set-up for Single-Shot analysis and operation procedure 4-7
4.3.2 Set-up for Double-Shot analysis and operation procedure 4-9
4.3.3 Set-up for Direct EGA analysis and operation procedure 4-12
4.3.4 Set-up for Heart-Cut EGA analysis and operation procedure 4-14
4.4 OTHER FUNCTIONS 4-17
4.4.1 Saving/loading analysis set-ups 4-17
4.4.2 Temperature calibration of pyrolyzer furnace and other set-ups 4-17
4.4.2.1 Temperature calibration of pyrolyzer furnace 4-18
4.4.2.2 Other set-ups for pyrolyzer furnace 4-19
4.4.2.3 Checking valve operations 4-19
4.4.2.4 Set-up MicroJet Cryo-Trap 4-19
4.4.3 Printing set-ups 4-20
4.4.4 Set-up the Py Conditioning Table 4-20
CHAPTER 5 FOUR ANALYSIS METHODS AND SAMPLE PREPARATION 5-1
5.1 SINGLE-SHOT ANALYSIS 5-1
5.2 EVOLVED GAS ANALYSIS (EGA) 5-3
5.3 DOUBLE-SHOT ANALYSIS 5-5
5.4 HEART-CUT ANALYSIS 5-7
5.5 SAMPLE PREPARATIONS 5-9
A-6
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A-7
Ver.1.09
CHAPTER 6 MAINTENANCE 6-1
6.1 ROUTINE MAINTENANCE 6-1
6.1.1 Cleaning sample cups (Eco-cup) 6-1
6.1.1.1 About reusing an Eco-cup F 6-1
6.1.1.2 Cleaning by red-heating 6-2
6.1.1.3 Solvent cleaning 6-2
6.1.2 Replacing and cleaning quartz pyrolysis tube 6-3
6.1.2.1 Replacing the quartz pyrolysis tube 6-3
6.1.2.2 Solvent cleaning 6-6
6.1.2.3 Flame cleaning with a torch 6-7
6.1.3 Interface needle 6-8
6.1.3.1 Clogging by sample contamination 6-8
6.1.3.2 Clogging by septum debris 6-8
6.1.4 GC injection port 6-9
6.1.4.1 Septa 6-9
6.1.4.2 Insert liner 6-9
6.1.4.3 Column 6-9
6.1.4.4 Absorption trap tube 6-9
6.2 REGULAR MAINTENANCE 6-10
6.2.1 Pyrolyzer furnace 6-10
6.2.2 GC 6-12
6.2.3 Temperature Controller 6-12
6.2.4 When not in use for a long period of time 6-12
6.2.5 List of recommended replacement parts 6-13
6.2.6 Periodic maintenance and inspection 6-14
6.3 ABOUT AVAILABILITY OF PARTS AND REPAIR ACCEPTANCE 6-14
CHAPTER 7 TROUBLESHOOTING 7-1
7.1 PYROLYZER FURNACE 7-1
7.2 TEMPERATURE CONTROLLER 7-3
7.3 TYPICAL TROUBLESHOOTING PROCEDURE 7-4
7.4 LIST OF ERROR CODES FROM COTROL SOFTWARE 7-6
CHAPTER 8 GUARANTEE OF BASIC PERFORMANCE (REPRODUCIBILITY) 8-1
CONSUMABLE PARTS LIST Appendix-1
LIST OF OPTIONAL PRODUCTS Appendix-3
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